Small Scale Approach to Organic Laboratory Techniques 4th Edition Pavia Solutions Manual
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Small Scale Approach to Organic Laboratory Techniques 4th Edition Pavia Solutions Manual.
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Product details:
- ISBN-10 : 1305253922
- ISBN-13 : 978-1305253926
- Author:
Featuring new experiments, a new essay, and new coverage of nanotechnology, this organic chemistry laboratory textbook offers a comprehensive treatment of laboratory techniques including small scale and some microscale methods that use standard-scale (\”macroscale\”) glassware and equipment. The book is organized based on essays and topics of current interest and covers a large number of traditional organic reactions and syntheses, as well as experiments with a biological or health science focus. Seven introductory technique-based experiments, thirteen project-based experiments, and sections on green chemistry and biofuels spark students’ interest and engage them in the learning process. Instructors may choose to offer Cengage Learning’s optional Premium Website, which contains videos on basic organic laboratory techniques.
Table of contents:
Introduction. WELCOME TO ORGANIC CHEMISTRY. Laboratory Safety. Organization of the Textbook. Advance Preparation. Budgeting Time. Purpose. PART I: INTRODUCTION TO BASIC LABORATORY TECHNIQUES. Experiment
1. Solubility. Experiment
2. Crystallization. Experiment
3. Extraction. Experiment
4. A Separation and Purification Scheme. Experiment 4A. Extractions with a Separatory Funnel. Experiment 4B. Extractions with a Screw-Cap Centrifuge Tube Experiment
5. Chromatography. Experiment 5A. Thin-Layer Chromatography. Experiment 5B. Selecting the Correct Solvent for Thin-Layer Chromatography. Experiment 5C. Monitoring a Reaction with Thin Layer Chromatography. Experiment 5D. Column Chromatography. Experiment
6. Simple and Fractional Distillation Experiment
7. Infrared Spectroscopy and Boiling-Point Determination Essay. Aspirin. Experiment
8. Acetylsalicylic Acid. Essay. Analgesics. Experiment
9. Acetaminophen. Essay. Identification of Drugs. Experiment 10.TLC Analysis of Analgesic Drugs. Essay. Caffeine. Experiment
11. Isolation of Caffeine. Experiment 11A. Extraction of Caffeine from Tea. Experiment 11B. Isolation of Caffeine from a Tea Bag. Essay. Esters–Flavors and Fragrances. Experiment
12: Isopentyl Acetate (Banana Oil). Essay, Terpenes and Phenylpropanoids. Experiment
13. Isolation of Eugenol from Cloves. Essay. Stereochemical Theory of Odor. Experiment
14. Spearmint and Caraway Oil: (+)- and (-)- Carvones. Essay.The Chemistry of Vision. Experiment
15. Isolation of Chlorophyll and Carotenoid Pigments from Spinach. Essay: Ethanol and Fermentation Chemistry. Experiment
16. Ethanol from Sucrose. PART II: INTRODUCTION TO MOLECULAR MODELING. Essay: Molecular Modeling and Molecular Mechanics. Experiment
17. An Introduction to Molecular Modeling. Experiment 17A. The Conformations of n-Butane: Local Minima. Experiment 17B. Cyclohexane Chair and Boat Conformations. Experiment 17C. Substituted Cyclohexane Rings (Critical Thinking Exercise). Experiment 17D. cis- and trans-2-Butene. Essay: Computational Chemistry – Ab initio and Semiempirical Methods. Experiment
18. Computational Chemistry. Experiment 18A. Heats of Formation: Isomerism, Tautomerism, and Regioselectivity. Experiment 18B. Heats of Reactions: SN1 Reaction Rates. Experiment 18C. Density-Electrostatic Potential. Maps: Acidities of Carboxylic Acids. Experiment 18D. Density -Electrostatic Potential Maps: Carbocations. Experiment 18E. Density -LUMO Maps: Reactivities of Carbonyl Groups. PART III: PREPARATIONS AND REACTIONS OF ORGANIC COMPOUNDS. Experiment
19. Reactivities of Some Alkyl Halides. Experiment
20. Nucleophilic Substitution Reactions: Competing Nucleophiles Experiment 20A. Competing Nucleophiles with 1-Butanol or 2-Butanol. Experiment 20B. Competing Nucleophiles with 2-Methyl-2-Propanol. Experiment 20C. Analysis. Experiment
21. Synthesis of n-Butyl Bromide and t-Pentyl Chloride. Experiment 21A. n-Butyl Bromide. Experiment 21B. t-Pentyl Chloride. Experiment
22. 4-Methylcyclohexen Essay. Fats and Oils. Experiment
23. Methyl Stearate from Methyl Oleate. Essay: Soap Experiment
24. Preparation of Soap. Essay: Petroleum and Fossil Fuels. Experiment
25. Gas Chromatographic Analysis of Gasolines. Essay: Biofuels. Experiment
26. Biodiesel. Experiment 26A. Biodiesel from Coconut Oil. Experiment 26B. Biodiesel from Other Oils. Experiment 26C. Analysis of Biodiesel. Essay: Green Chemistry. Experiment
27. Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination. Experiment 27A. Chiral Reduction of Ethyl Acetoacetate. Experiment 27B. NMR Determination of the Optical Purity of Ethyl (S)-3-Hydroxybutanoate. Experiment
28. Nitration of Aromatic Compounds Using a Recyclable Catalyst. Experiment
29. Reduction of Ketones Using Carrots as Biological Reducing Agents Experiment
30. Resolution of (+/-)-alpha-Phenylethylamine and Determination of Optical Purity. Experiment 30A. Resolution of (+/-)-alpha-Phenylethylamine. Experiment 30B. Determination of Optical Purity Using NMR and a Chiral Resolving Agent. Experiment
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